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YS/T 1085-2015 English PDF (YST1085-2015)

YS/T 1085-2015 English PDF (YST1085-2015)

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YS/T 1085-2015: Refined nickel. Determination of Silicon, manganese, phosphorus, iron, copper, cobalt, magnesium, aluminum, zinc, chromium. Inductively coupled plasma atomic emission spectrometric method
This standard specifies the method for the determination of silicon, manganese, phosphorus, iron, copper, cobalt, magnesium, aluminum, zinc and chromium content in refined nickel by using an inductively coupled plasma atomic emission spectrometric method. This method is applicable to the analysis of silicon, manganese, phosphorus, iron, copper, cobalt, magnesium, aluminum, zinc and chromium content in refined nickel. The measuring range of each element is shown in Table 1. Table 1 -- Measuring range of each element Element Measuring range (mass fraction)/% YS/T 1085-2015 www.ChineseStandard.net ? Buy True-PDF ? Auto-delivery Page 5 of 16 2 Method principle A certain amount of the sample is weighed and decomposed by the nitric acid; an inductively coupled plasma atomic emission spectrometer is used to measure the spectral intensity of the spectral line of the element to be measured in the solution; the spectral line is corrected by subtracting the background to eliminate the influence of the matrix nickel; the elemental content is obtained from the calibration curve drawn according to the standard solution. 3 Reagents Unless otherwise stated, the reagents used in this standard are all of analytical grade, and the water used is first-grade water. 3.1 Nitric acid (¦Ñ=1.42 g/mL). 3.2 Nitric acid (1+1). 3.3 Hydrofluoric acid (¦Ñ=1.15 g/mL). 3.4 Silicon standard stock solution: Heat high-purity silica (the content is greater than 99.9%) at a temperature of 1100 ¡ãC until its mass is constant, and cool to room temperature in a desiccator; weigh 2.1393 g and put it into a platinum crucible, add about 5 g of sodium carbonate, heat and melt for 15 minutes. Take it out and cool it slightly, place it in a 500 mL beaker, dissolve the melt with water, and wash out the platinum crucible; then, transfer the solution into a 1000 mL volumetric flask, wash the beaker with water and pour the washing liquid into the volumetric flask, add water to the scale of the volumetric flask, mix...

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