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GB/T 7702.8-2008 English PDF (GBT7702.8-2008)

GB/T 7702.8-2008 English PDF (GBT7702.8-2008)

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GB/T 7702.8-2008: Test method for granular activated carbon from coal -- Determination of phenol adsorption

This Part specifies the principle, procedures, result calculation and other related contents for determination of phenol adsorption of granular activated carbon from coal. This Part is applicable to determination of phenol adsorption of granular activated carbon from coal. It is also applicable to powdery activated carbon from coal.
GB/T 7702.8-2008
GB
ICS 75.160.10
D 24
NATIONAL STANDARD
OF THE PEOPLE REPUBLIC OF CHINA
Replacing GB/T 7702.8-1997
Test Method for Granular Activated Carbon from
Coal - Determination of Phenol Adsorption
ISSUED ON. FEBRUARY 1, 2008
IMPLEMENTED ON. JULY 1, 2008
Jointly issued by. General Administration of Quality Supervision,
Inspection and Quarantine (AQSIQ);
Standardization Administration (SAC) of the PEOPLE
Republic of China.
Table of Contents
Foreword ... 3
1 Scope ... 5
2 Normative References... 5
3 Terms and Definitions ... 6
4 Principle ... 6
5 Reagents and Materials ... 6
6 Instruments and Apparatuses ... 7
7 Sample Preparation ... 8
8 Determination Procedures ... 8
9 Result Calculation ... 8
10 Precision ... 9
11 Test Report ... 9
Foreword
Test Method for Granular Activated Carbon from Coal" (GB/T 7702) is divided into. ?€? Part 1. Determination of Moisture;
?€? Part 2. Determination of Particle Size;
?€? Part 3. Determination of Hardness;
?€? Part 4. Determination of Packing Density;
?€? Part5. Determination of Absorption of Water;
?€? Part 6. Determination of Methylene Blue Absorption;
?€? Part 7. Determination of Iodine Number;
?€? Part 8. Determination of Phenol Absorption;
?€? Part 9. Determination of Ignition Temperature;
?€? Part 10. Determination of Service Life against Benzene and Chloroethane Vapors;
?€? Part 13. Determination of CCL4 Vapor Absorption;
?€? Part14. Determination of Sulphur Capacity;
?€? Part 15. Determination of Ash Content;
?€? Part 16. Determination of pH Value;
?€? Part 17. Determination of Floatation Ratio;
?€? Part 18. Determination of Caramel Absorption;
?€? Part 19. Determination of Carbon Tetrachloride (CCl4) Desorption;
?€? Part 20. Determination of Pore Volume and Specific Surface Area.
This Part is Part 8 of GB/T 7702.
This Part replaces GB/T 7702.8-1997 "Standard Test Method for Phenol Adsorption of Granular Activated Carbon from Coal - Determination of Phenol Absorption". Compared with GB/T 7702.8-1997, the main changes of this Part are as follows. a) Specify the requirements of water for laboratory use;
b) Specify the grade and specification of filter paper for analysis ;
c) Add the refining method for phenol;
d) Specify the specimen weighing range. Increase the weighing accuracy; e) Add Chapter 3 - "Terms and Definitions".
This Standard was proposed by and shall be under the jurisdiction of China North Industries Group Corporation.
Drafting organization of this Standard. Shanxi Xinghua Chemical Co., Ltd. Main drafting staffs of this Standard. Cheng Qingjun, Yuan Yidong, Zhang Xu, Li Weibing, Pang Huisheng, Chi Guangxiu, and Li Ruomei.
This Standard was issued in 1987 for the first time, and revised in 1997 for the first time.
NATIONAL STANDARD
OF THE PEOPLE REPUBLIC OF CHINA
Replacing GB/T 7702.8-1997
Test Method for Granular Activated Carbon from Coal -
Determination of Phenol Adsorption
1 Scope
This Part specifies the principle, procedures, result calculation and other related contents for determination of phenol adsorption of granular activated carbon from coal.
This Part is applicable to determination of phenol adsorption of granular activated carbon from coal. It is also applicable to powdery activated carbon from coal. 2 Normative References
The following standards contain provisions which, through reference in this text, constitute provisions of this Part of GB/T 7702. For dated reference, the subsequent amendments (excluding correction) or revisions of these publications do not apply. However, the parties who enter into agreement based on this standard are encouraged to investigate the possibility of applying the most recent editions of the standards. For undated references, the latest edition of the normative document referred to applies.
GB/T 601-2002 Chemical Reagent - Preparations of Standard Volumetric
Solutions
GB/T 622 Chemical Reagent - Hydrochloric Acid (GB/T 622-2006, ISO
6353-2.1983, NEQ)
GB/T 649 Chemical Reagent - Potassium Bromide
GB/T 650 Chemical Reagents - Potassium Bromate (GB/T 650-1993, neq ISO
6353-3.1987 R75)
GB/T 1272 Chemical Reagent - Potassium Iodide (GB/T 1272-2007, ISO
Where,
c ?€? The concentration of sodium thiosulfate standard titration solution, in mol/L; V1 ?€? The volume of sodium thiosulfate standard titration solution consumed by specimen titration, in mL;
V2 ?€? The volume of sodium thiosulfate standard titration solution consumed by titration in blank test, in mL;
M ?€? The molar mass of phenol [M(1/6C6H5OH)=15.68 g/mol], in g/mol;
m ?€? The mass of specimen, in g.
10 Precision
Parallel determination shall be carried out for each test sample by using 2 portions of specimens. The difference of 2 determination results, expressed by arithmetic mean, shall not be more than 2% (2% of the mean value). The calculation results shall be rounded off to integer.
11 Test Report
The test report shall include the following contents.
a) Serial number of the sample;
b) The standards used;
c) The methods used;
d) Test items;
e) Test results;
f) Testing personnel;
g) Date of test.

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