GB/T 5009.162-2008: Determination of organochlorine pesticide and pyrethroid pesticide multiresidues in animal original foods

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Scope

The method-1 of this standard specifies the determination method for the
chromatography-mass spectrometry (GC-MS) of benzenehexachloride, DDT,
hexachlorobenzene, heptachlor, heptachlor epoxide, chlordane, aldrin, dieldrin,
endrin, mirex, pentachloronitrobenzene, endosulfan, fenson, allethrin,
dichlorophenyl benzensulfonate, tetramethrin, fenpropathrin, permethrin,
cypermethrin, fenralerate, deltamenthrin.
The method-2 of this standard spcifies the determination method of gas
chromatography-electron capture device (GC-ECD) for the
benzenethexzchloride, DDT, pentachloronitrobenzene, heptachlor, heptachlor
epoxide, aldrin, dieldrin, fenson, ovex, tetramethrin, permethrin, cypermethrin,
α-fenralerate, deltamethrin.
The method-1 of this standard applies to the confirmation analysis of α-
benzenehexachloride, hexachlorobenzene, β-benzenehexachloride, γ-
benzenehexachloride, pentachloronitrobenzene, δ-benzenehexachloride,
pentachloraniline, heptachlor, pentachlorophenyl sulfide, aldrin, oxychlordane,
heptachlor epoxide, trans-chlordane, α-endosulfan, cis-chlordane, p,p’-DDE,
dieldrin, endrin, β-endosulfan, p,p’-DDD, o,p’-DDT, endrin aldehyde,
endosulfan sulfate, p,p’-DDT, endrin ketone, mirex, fenson, allethrin, 2,4-
dichlorophenyl benzensulfonate, ovex, tetramethrin, fenpropathrin, permethrin,
cypermethrin, fenralerate, deltamenthrin in meat, egg, milk food, fat (including
vegetable oil).
The method-2 of this standard applies to the analysis of 20 commonly-used
organochlorine pesticides and pyrethroid pesticide residues such as α-
benzenehexachloride, β-benzenehexachloride, γ-benzenehexachloride, δ-
benzenehexachloride, pentachloronitrobenzene, heptachlor, heptachlor
epoxide, aldrin, dieldrin, fenson, ovex, p,p’-DDE, p,p’-DDD, o,p’-DDT, p,p’-DDT,
tetramethrin, permethrin, cypermethrin, α-fenralerate, deltamenthrin.
The detection limits (µg/kg) of various pesticides in method-1 of this standard
are: α-benzenehexachloride 0.20; hexachlorobenzene 0.20; β-
benzenehexachloride 0.20; γ-benzenehexachloride 0.20;
pentachloronitrobenzene 0.50; δ-benzenehexachloride 0.20; pentachloraniline
0.50; heptachlor 0.50; pentachlorophenyl sulfide 0.50; aldrin 0.50;
oxychlordane 0.20; heptachlor epoxide 0.50; trans-chlordane 0.20; α-
endosulfan 0.50; cis-chlordane 0.20; p,p’-DDE 0.20; dieldrin 0.20; endrin 0.50;
β-endosulfan 0.50; p,p’-DDD 0.20; o,p’-DDT 0.20; endrin aldehyde 0.50;
endosulfan sulfate 0.50; p,p’-DDT 0.20; endrin ketone 0.50; mirex 0.20; fenson
0.50; allethrin 0.50; 2,4-dichlorophenyl benzensulfonate 0.50; ovex 0.50;
tetramethrin 1.00; fenpropathrin 1.00; permethrin 1.00; cypermethrin 2.00;
fenralerate 2.00; deltamenthrin 2.00.
The detection limits (µg/kg) of various pesticides in method-2 of this standard
are: α-benzenehexachloride 0.25; β-benzenehexachloride 0.50; γ-
benzenehexachloride 0.25; δ-benzenehexachloride 0.25;
pentachloronitrobenzene 0.25; heptachlor 0.50; heptachlor epoxide 0.50; aldrin
0.25; dieldrin 0.50; fenson 1.25; ovex 1.25; p,p’-DDT 0.50; o,p’-DDT 0.50; p,p’-
DDE 0.60; p,p’-DDD 0.75, tetramethrin 12.50; permethrin 7.50; cypermethrin
2.00; α-fenralerate 2.50; deltamenthrin 2.50.
Method-1 -- Gas chromatography-mass spectrometry

Basic Data

Standard ID	GB/T 5009.162-2008 (GB/T5009.162-2008)
Description (Translated English)	Determination of organochlorine pesticide and pyrethroid pesticide multiresidues in animal original foods
Sector / Industry	National Standard (Recommended)
Classification of Chinese Standard	C53
Classification of International Standard	67.040
Word Count Estimation	21,299
Date of Issue	2008-12-03
Date of Implementation	2009-03-01
Older Standard (superseded by this standard)	GB/T 5009.162-2003
Regulation (derived from)	National Standard Approval Announcement 2008 No.22 (Total No.135)
Issuing agency(ies)	General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary	This standard specifies the animal foods BHC, DDT, HCB, heptachlor, heptachlor epoxide, chlordane, Aldrin, dieldrin, endrin, mirex, pentachlorophenol nitro benzene, endosulfan, mites ester, allethrin, acaricidal sulfur, acaricidal ester, tetramethrin, fenpropathrin, permethrin, cypermethrin, fenvalerate, deltamethrin gas chromatography-mass spectrometry (GC-MS) spectrometry. The second law provides a standard animal foods BHC, DDT, PCNB, heptachlor, heptachlor epoxide, Aldrin, dieldrin, mites ester, Acaricidal ester, Tetramethrin, electron capture detector (GC-ECD) determination, permethrin, cypermethrin, ��- fenvalerate, deltamethrin gas chromatography. This standard is the first law applies to meat, eggs, dairy foods.