GB/T 18932.24-2005: Method for the determination of the metabolite residues of furaltadon, nitrofurazone, nitrofurantoin and furazolidone in honey - Liquid chromatography-tandem mass spectrometry method

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Scope

This Part of GB/T 18932 specifies the liquid chromatography - tandem mass
spectrometry determination method for the metabolite residues of 5-methylmorpholine-
3-amino-2-yl alkyl ketones in furaltadon, semicarbazide in nitrofurazone, 1-amino-2-
hydantoin in nitrofurantoin and 3-amino-2-yl alkyl ketones in furazolidone in honey.
This Part applies to the determination of the residues of 5-methylmorpholine-3-amino-
2-yl alkyl ketones, semicarbazide, 1-amino-2-hydantoin and 3-amino-2-yl alkyl ketones
in honey.
The detection limit of the method in this Part. 0.2μg/kg for 5-methylmorpholine-3-
amino-2-yl alkyl ketones and 3-amino-2-yl alkyl ketones; 0.5μg/kg for semicarbazide
and 1-amino-2-hydantoin.

Basic Data

Standard ID	GB/T 18932.24-2005 (GB/T18932.24-2005)
Description (Translated English)	Method for the determination of the metabolite residues of furaltadon, nitrofurazone, nitrofurantoin and furazolidone in honey - Liquid chromatography-tandem mass spectrometry method
Sector / Industry	National Standard (Recommended)
Classification of Chinese Standard	X31
Classification of International Standard	67.180.10
Word Count Estimation	10,168
Date of Issue	2005-02-04
Date of Implementation	2005-08-01
Quoted Standard	GB/T 6379; GB/T 6682;
Regulation (derived from)	Announcement of Newly Approved National Standards No. 4 of 2005 (total 78)
Issuing agency(ies)	General Administration of Quality Supervision, Inspection and Quarantine of the People Republic of China, China National Standardization Administration Committee
Summary	This standard specifies: honey furaltadone metabolite 5 methyl morpholin-3 amino-2 yl alkyl ketones, nitrofurazone metabolite semicarbazide, nitrofurantoin Metabolic object 1 amino-2 the acid urea and furanone metabolite, 3 amino-2 yl alkyl ketone residues in liquid chromatography tandem mass spectrometry Determination. This standard applies to: Honey 5 methyl morpholin-3 amino-2 yl alkyl ketones, semicarbazide 1 amino-2 hydantoin 3 amino-2 yl alkyl ketones Residues determination. This standard method detection limit