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GB 13078-2001 English PDF (GB13078-2001)

GB 13078-2001 English PDF (GB13078-2001)

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GB 13078-2001: Hygienical standard for feeds

This Standard specifies the allowable amount of harmful substances and microorganisms in feeds, feed additives products as well as test methods.
GB 13078-2001
GB
NATIONAL STANDARD OF
THE PEOPLE REPUBLIC OF CHINA
ICS 65.120
B 46
Replacing GB 13078-1991
Hygienical standard for feeds
ISSUED ON. JULY 20, 2001
IMPLEMENTED ON. OCTOBER 1, 2001
Issued by. General Administration of Quality Supervision, Inspection
and Quarantine of China
Table of Contents
Foreword ... 3
1 Scope ... 5
2 Normative references ... 5
3 Requirements ... 6
Amendment No. 1 ... 12
Foreword
All technical contents of this Standard are mandatory.
This Standard is a modification and supplement to GB 13078-1991 Hygienical standards for feeds.
Compared with GB 13078-1991, the main technical differences in this Standard are as follows.
- according to the objective needs of feed products, it allowed an increase of amount of indicators of chromium in the feed, feed additives;
- added a supplementary provision on arsenic tolerance indicator in feed additives and pig, poultry feed premix feed and concentrate feed, cattle, sheep concentrate supplement products; modified the permissible amount
of arsenic in phosphate products from 10 mg/kg to 20 mg/kg;
- added a supplementary provision on the allowable amount of lead in duck compound feed, bovine concentrate supplement, chicken, pig
concentrated feed, bone powder, meat and bone powder, chicken and pig
compound premix;
- modified the permissible amount of fluorine in dicalcium phosphate
products from 2000 mg per kilograms to 1800 mg per kilograms; added a
supplementary provision on the allowable amount of fluorine in bone
powder, meat and bone powder, duck feed, cattle concentrate supplement, pig, poultry additives premixed feed, laying hen, pig, poultry concentrated feed products;
- added a supplementary provision on the allowable amount of mold in
bean cake (dregs), rapeseed cake (dregs), fish powder, meat and bone
powder, pig, chicken, duck feed, pig, chicken concentrated feed, bovine feed supplement material products;
- in aflatoxin B1 health indicators, broiler feed is divided into pre-feed and later feed of which the allowable values were respectively revised to 10 ??g and 20 ??g per kilograms of feed; added a supplementary provision on
he allowable amount of aflatoxin B1 in cottonseed cake (dregs), rapeseed cake (dregs), bean dregs, piglet, pig feed and concentrated feed, chick compound feed, chick, chicken, growing chicken, laying hen concentrated feed, duck feed and concentrated feed, quail compound feed and
concentrated feed, bovine feed supplement materials;
- added a supplementary provision on test methods for health indicators. Hygienical standard for feeds
1 Scope
This Standard specifies the allowable amount of harmful substances and micro- organisms in feeds, feed additives products as well as test methods.
This Standard is applicable to the feeds, feed additives products irrespective of types listed in Table 1.
2 Normative references
The following standards contain the provisions which, through reference in this Standard, constitute the provisions of this Standard. At the time of publication of this Standard, the versions shown are valid. All standards shall be revised. However, the parties who enter into agreement based on this Standard are encouraged to investigate whether the latest versions of these documents are applicable.
GB/T 8381-1987, Aflatoxin B1 in animal feeding stuffs - Semi-quantitative thin layer chromatographic methods (neq ISO 6651.1987)
GB/T 13079-1999, Determination of total arsenic in feeds
GB/T 13080-1991, Determination of lead in feeds - Method using atomic
absorption spectrometry
GB/T 13081-1991, Method for determination of mercury in feeds
GB/T 13082-1991, Method for determination of cadmium in Feeds
GB/T 13083-1991, Method for determination of fluorine in feeds
GB/T 13084-1991, Method for determination of glycosidic hydrocyanic acid in feeds
GB/T 13085-1991, Determination of nitrite in feed - Method using colorimetric analysis
GB/T 13086-1991, Method for determination of free gossypol in feeds
GB/T 13087-1991, Method for determination of isothiocyanates in feeds
GB/T 13088-1991, Method for determination of chromium in feeds
GB/T 13089-1991, Method for determination of oxazolidinethione in feeds GB/T 13090-1991, Method for determination of bhc and ddt in feeds
GB/T 13091-1991, Determination of Salmonella in feeds
GB/T 13092-1991, Method for determination of Molds in feeds
GB/T 13093-1991, Method for determination of aerobic bacterial count in feeds
GB/T 17480-1998, Determination of aflatoxin B1 in feeds - Enzyme-linked immunosorbent assay (eqv AOAC method)
HG 2636-1994, Dicalcium phosphate of feed grade
3 Requirements
Health indicators and test methods for feeds, feed additives are listed in Table 1.
Table 1 Health indicators for feeds, feed additives
S/N Health indicator item Product name Indicator Test method Remark
The allowable amount
(in per kilograms) of
arsenic (in total
arsenic)
mg
Stone powder
??? 2.0
GB/T 13079
Excluding the
content of arsenic
in organic arsenic
formulations
approved by
national authorities
Ferrous sulfate,
magnesium sulfate
Phosphate ??? 20.0
Zeolite powder,
bentonite, medical
stone
??? 10.0
Copper sulphate,
manganese sulphate,
zinc sulphate,
potassium iodide,
calcium iodate, cobalt
chloride
??? 5.0
Zinc oxide ??? 10.0
Fish powder, meat
powder, meat and bone
powder
??? 10.0
Poultry, pig compound
feed ??? 2.0
Growing duck, meat-
type duck compound
feed
??? 200
Laying duck compound
feed ??? 250
Cattle (cow, beef cattle)
concentrate
supplementary feed
??? 50
Pig, poultry additives
premixed feed ??? 1000
GB/T 13083
Based on 1% of the
amount added in
compound feed
Pig, poultry
concentrated feed
After
conversion
according to
the
appending
proportion, it
is same with
correspondin
g specified
values of pig,
poultry
compound
feed
The allowable amount
(in per kilograms) of
mold
Total number of
molds ?? 103
Corn
< 40
GB/T 13092
Limited feeding. 40
~ 100
Forbidden. > 100
Wheat bran, rice bran
Limited feeding. 40
~ 80
Forbidden. > 80
Bean cake (dregs),
cottonseed cake
(dregs), rapeseed cake
(dregs)
< 50
Limited feeding. 50
~ 100
Forbidden. > 100
Fish powder, meat and
bone powder < 20
Limited feeding. 20
~ 50
Forbidden. > 50
Duck compound feed < 35
Pig, chicken compound
feed
Pig, chicken
concentrated feed
< 45
The allowable amount
(in per kilograms) of
mercury (in Hg)
mg
Stone powder
Chicken compound
feed, pig compound
feed
??? 0.1
The allowable amount
(in per kilograms) of
chromium (in Cd)
mg
Rice bran ??? 1.0
GB/T 13082
Fish powder ??? 2.0
Stone powder ??? 0.75
Chicken compound
feed, pig compound
feed
??? 0.5
The allowable amount
(in per kilograms) of
cyanide (in HCN)
mg
Dried cassava ??? 100
GB/T 13084 Flax cake, dregs ??? 350
Chicken compound
feed, pig compound
feed
??? 50
The allowable amount
(in per kilograms) of
nitrite (in NaNO2)
mg
Fish powder ??? 60
GB/T 13085 Chicken compound feed, pig compound
feed
??? 15
The allowable amount
(in per kilograms) of
free gossypol
mg
Cottonseed cake, dregs ??? 1200
GB/T 13086
Broiler chicken, growing
chicken compound feed ??? 100
Laying hen compound
feed ??? 20
Growing and finishing
pig compound feed ??? 60
The allowable amount
(in per kilograms) of
Isothiocyanate (in
propenyl
isothiocyanate)
mg
Rapeseed cake, dregs ??? 4000
GB/T 13087 Chicken compound
feed
Growing and finishing
pig compound feed
??? 500
The allowable amount
(in per kilograms) of
oxazolidinethione
mg
Broiler chicken, growing
chicken compound feed ??? 1000 GB/T 13089 Laying hens compound
feed ??? 500
14 Rice bran Wheat bran ??? 0.05 GB/T 13090
Amendment No. 1
GB 13078-2001 Hygienical standard for feeds
This Amendment was approved by National Standardization Administration
Committee on November 11, 2003 remarked as No. 97 Letter of National
Standard Committee Agricultural Light Industry [2003] and implemented since April 1, 2004.
1. The product name of ?€?1 (arsenic)?€? in Table 1 is divided into four categories, of which ?€?the feed product added with organic arsenic?€? is a new addition. It also specifies the allowable amount of total arsenic.
2. Deleted the contents of the remark column of ?€?1 (arsenic)?€?, ?€?2 (lead)?€?, ?€?3 (fluorine)?€?.
3. Modified the phosphate test method in ?€?3 (fluorine)?€? of Table 1 to GB/T 13083. It made a slight change on the provision statement of pig poultry concentrated feed indicators.
4. Modified NOTE 1, 2 at the end of Table 1 to. a refers that the use method and amount of organic arsenic preparation approved by national authorities shall comply with the provisions of relative documents. For feed product added with organic arsenic preparation, it should mark the accurate content of organic arsenic on the label (calculated according to actual added
amount).
The modified 1 (arsenic), 2 (lead), 3 (fluorine) and the note in the end column of Table 1 are as follows.
Table 1 Health indicators for feeds, feed additives
S/N
Health
indicator
item
Product name Indicator Test method Remark
The allowable
amount (in per
kilograms) of
arsenic (in total
arsenic) / mg
Mineral feed ...

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